Abstract
ZrCl 4 which is commercially available and not a costly compound, is a relatively safe chemical [LD 50 [ZrCl 4, oral rat] = 1688 mg Kg]. In this report we describe the use of ZrCl 4 dispersed on dry silica gel as an efficient reagent for the efficient preparation of thioethers from thiols with alcohols under solvent-free conditions.
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