Vertical electropolishing for 1.3 GHz single- and nine-cell superconducting niobium cavities: A parametric optimization and rf performance

Abstract

Electropolishing (EP) is a standard process for the treatment of the interior surface of niobium (Nb) superconducting radio-frequency (SRF) cavities used in particle accelerators. We previously conducted a study on vertical electropolishing (VEP), in which the cavity was set vertically during EP of a 1.3 GHz Nb single-cell cavity. In that study, we showed that the major cause of asymmetric removal in VEP is the accumulation of hydrogen gas bubbles, generated during the EP process, on the upper half cell of the cavity. Three types of unique rotating cathodes were tested with the aim to resolve the issues of asymmetric removal and rough surface. Appropriate cathode design and parameters reduced the asymmetric removal in the cell and yielded a smooth surface of the cavity. In this study, we have performed an extensive investigation on VEP of both single- and nine-cell Nb 1.3 GHz cavities with a modified cathode. The VEP parameters with single- and nine-cell coupon cavities were investigated, which facilitate an in situ study of the coupon currents at various positions of the cavities and observation from the viewports located near the iris and equator positions of the cavities. The modified cathode and optimized VEP process for the single-cell cavity yielded uniform removal in the cavity cell and a smooth surface of the interior of the cavity. A novel acid flow method that allows the separation of the acid flow in the cavity and cathode housing was employed in the nine-cell cavity to efficiently remove the gas bubbles from the cavity. The optimized acid flow rates in the cavity and cathode housing, along with other adequate parameters including temperature, cathode rotation speed, and applied voltage, made the surface smooth and significantly reduced the removal nonuniformity in the nine-cell cavity. The single- and nine-cell cavities after an average removal of 46 and $130\text{ }\text{ }\ensuremath{\mu}\mathrm{m}$, respectively, were tested in a vertical cryostat. The single- and nine-cell cavities achieved $31\text{ }\text{ }\mathrm{MV}/\mathrm{m}$ at a ${Q}_{0}$ value of $9\ifmmode\times\else\texttimes\fi{}{10}^{9}$ and $28.3\text{ }\text{ }\mathrm{MV}/\mathrm{m}$ at a ${Q}_{0}$ value of $6.7\ifmmode\times\else\texttimes\fi{}{10}^{9}$, respectively, in the rf tests at the temperature of 2 K. The achieved SRF performances were as good as the baseline performances achieved after the horizontal electropolishing process of the same cavities.