Abstract
An oven microwave was established for synthesis of zinc oxide nanoparticles using Sargassum sp. and Padina sp. extract and 0.1 M ZnCl2 solution as a precursor. The ZnO nanoparticles had been characterized such as chemical structure by Fourier transform infrared (FTIR) spectroscopy, particle size distribution with Particle Size Analyzer (PSA), Scanning Electron Microscopy-Energy Dispersive Spectroscopy (SEMEDS) and crystalline properties with X-ray diffraction (XRD). The result showed that FTIR spectra revealed the involvement of hydroxyl groups and sulfate polysaccharide in the formation of ZnO NPs and protein was involved in stabilizing. PSA analysis showed that the size ranged of ZnO NPs extract Sargassum sp. synthesized 351,14 and 1.336.19 nm for extract Padina sp. The particle size distribution was homogeneous but their size hadn’t met the size of nanometers. The range of %mass elements Zn and O ZnO extract Sargassum sp. and Padina sp. synthesized didn’t approach standard ZnO. The crystallinity properties showed only ZnO extract of Padina sp. synthesized which had a peak with an angle value of 2θ was almost equal to standard ZnO and after confirmed to Match program! 3 crystal structure ZnO synthesized wasn’t imperfect hexagonal wurtzite. Ovens microwave could be used to synthesize ZnO from Padina sp. extract but it was still necessary to develop a method so that ZnO could be obtained with nanoparticle size and ideal hexagonal wurtzit structure.
Highlights
An oven microwave was established for synthesis of zinc oxide nanoparticles using Sargassum sp. and Padina sp. extract and 0.1 M ZnCl2 solution as a precursor
The ZnO nanoparticles had been characterized such as chemical structure by Fourier transform infrared (FTIR) spectroscopy, particle size distribution with Particle Size Analyzer (PSA), Scanning Electron Microscopy-Energy Dispersive Spectroscopy (SEMEDS) and crystalline properties with X-ray diffraction (XRD)
PSA analysis showed that the size ranged of ZnO NPs extract Sargassum sp. synthesized 351,14 and 1.336.19 nm for extract Padina sp
Summary
Bahan yang digunakan adalah rumput laut coklat Sargassum sp. dan Padina sp. dari perairan Binuangeun, Banten Selatan. Bahan yang digunakan adalah rumput laut coklat Sargassum sp. Rumput laut setelah dipanen dicuci dengan air laut, dibilas dan dikemas dalam coolbox yang berisi es curah lalu dibawa ke Balai Besar Pengolahan Produk dan Bioteknologi Kelautan dan Perikanan, Jakarta. Rumput laut dicuci kembali dengan air tawar dan dikering-anginkan selama seminggu sampai kadar airnya 12-17% (bk), selanjutnya digiling menjadi tepung. Bahan kimia yang digunakan ZnCl2 (Merck), NaOH (Merck), dan HCl (Merck), ZnO standar (Sigma aldrich), KBr (Merck) dan etanol (Merck). Alat yang digunakan yaitu coolbox (Marina Cooler) kapasitas 500 liter, hammer mill, hot plate (Labinco LD-844), freeze dryer (Christ Beta 2-8 LD plus), type pH meter009(I), oven microwave daya 399 W (Sharp) dan oven vacuum (Shellab). Peralatan analisis meliputi: instrumentasi scanning electron microscopy-energy dispersive spectroscopy/ SEM-EDS (Jeol), fourier transform infrared spectroscopy/FT-IR (Spectrophotometers Perkin Elmer), Particle Size Analyzer/PSA (Beckman Coulter), dan X-ray Diffraction/ XRD (Shimadzu XRD-7000 Maxima)
Sign-in/Register to view highlights & summary Sign-in/Register to access full text options 
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
