Abstract
Two three-dimensional coordination polymers were solvothermally prepared through in situ formation of a 2-sulfobenzoic acid ligand from a 2,2′-dithiobisbenzoic acid precursor involving the oxidative cleavage of its disulfide bond. Complex 1 shows neb-e topology, while complex 2 exhibits a scarcely reported twisting chiral dense 75.9 net.
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