Titanocene(III) mediated 8- endo radical cyclizations for the synthesis of eight-membered cyclic ethers

Samir Kumar Mandal,Subhas Chandra Roy

doi:10.1016/j.tetlet.2005.12.131

Titanocene(III) mediated 8- endo radical cyclizations for the synthesis of eight-membered cyclic ethers

Samir Kumar Mandal, Subhas Chandra Roy

https://doi.org/10.1016/j.tetlet.2005.12.131

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Journal: Tetrahedron Letters	Publication Date: Jan 20, 2006
Citations: 25

Affiliation: Indian Association for the Cultivation of Science

#Cp 2TiCl #Activated Zinc Dust + Show 7 more

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Abstract

Titanocene(III) chloride (Cp 2TiCl) mediated 8- endo radical cyclizations towards the synthesis of eight-membered cyclic ethers have been described. Titanocene(III) chloride was prepared in situ from commercially available titanocene dichloride (Cp 2TiCl 2) and activated zinc dust in THF.

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