Abstract
The selective dibutyltin oxide-mediated benzoylation of methyl 4,6- O-benzylidene-α- d-glucopyranoside at position 2 is not a post-acylation phenomenon as is the case with the equivalent benzoylation of phenylethyleneglycol. 1H NMR temperature studies have shown that such equilibration occurs only above 85°C in toluene- d 8 for the glucopyranoside.
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