Abstract

The compounds PSI and P 2SI 4 cannot be prepared by the methods claimed in the literature, the usual reaction product being a mixture of tetraphosphorus trithiodi-iodide, P 4S 3I 2, tetraphosphorus heptasulphide and phosphorus iodides. P 4S 3I 2 may be obtained in high yield from the elements in correct proportions.

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