Abstract
The thermal decomposition of complex salts of thiocyanatothiocarbamidobismuthates(III), having the general formula Me[Bi(SCN) 4(TM) 2] where Me = Li, Na, K, Rb, Cs, NH 4 and TM = thiourea, was studied. On the basis of the results of derivatographic studies and chemical analysis, both infrared spectrophotometric and diffractometric, the compositions of the intermediate and final products obtained during the thermal decomposition of those salts were established. On the strength of the experimental data obtained (without analyzing the gaseous products), the most probable overall equation was established of the decomposition reaction of thiocyanatothiocarbamidobismuthates(III) in air at a temperature of 480°C.
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