Abstract

The noise of the frequency-shift signal Δf in noncontact atomic force microscopy (NC-AFM) consists of cantilever thermal noise, tip–surface-interaction noise and instrumental noise from the detection and signal processing systems. We investigate how the displacement-noise spectral density dz at the input of the frequency demodulator propagates to the frequency-shift-noise spectral density dΔf at the demodulator output in dependence of cantilever properties and settings of the signal processing electronics in the limit of a negligible tip–surface interaction and a measurement under ultrahigh-vacuum conditions. For a quantification of the noise figures, we calibrate the cantilever displacement signal and determine the transfer function of the signal-processing electronics. From the transfer function and the measured dz, we predict dΔf for specific filter settings, a given level of detection-system noise spectral density dzds and the cantilever-thermal-noise spectral density dzth. We find an excellent agreement between the calculated and measured values for dΔf. Furthermore, we demonstrate that thermal noise in dΔf, defining the ultimate limit in NC-AFM signal detection, can be kept low by a proper choice of the cantilever whereby its Q-factor should be given most attention. A system with a low-noise signal detection and a suitable cantilever, operated with appropriate filter and feedback-loop settings allows room temperature NC-AFM measurements at a low thermal-noise limit with a significant bandwidth.

Highlights

  • In this contribution, we discuss noise in frequency-modulation noncontact atomic force microscopy (NC-AFM) using cantilevers as force sensors and optical beam deflection (OBD) for signal detection

  • We find that by the correct choice of the cantilever, by using optimised detection electronics and by appropriate phase-locked loop (PLL) filter settings, the frequency-shift signal Δf can be detected at a low thermal-noise limit over a bandwidth B that is more than 100 Hz for room temperature operation under UHV conditions

  • For a study on how the noise of the detection system propagates through the demodulation system, different noise levels are artificially created by using white noise from a waveform generator DS345 (Stanford Research Systems, Inc., Sunnyvale, CA, USA) added to the displacement signal Vz

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Summary

Introduction

We discuss noise in frequency-modulation noncontact atomic force microscopy (NC-AFM) using cantilevers as force sensors and optical beam deflection (OBD) for signal detection. A system with a low-noise signal detection and a suitable cantilever, operated with appropriate filter and feedback-loop settings allows room temperature NC-AFM measurements at a low thermal-noise limit with a significant bandwidth.

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