Abstract
The course of the thermal decomposition of APM was studied in vacuo and in air or argon atmosphere. The differences between vacuum and atmospheríc pressure decompositions were pointed out. The substantial participation of redox reactions in the vacuum decomposition was observed. The course of the vacuum decomposition was described in detail as a result of sensitive continuous analysis of the gaseous products. The final product of the vacuum decomposition is a mixture of lower molybdenum oxides. In the presence of oxygen the MoO3 obtained is only slightly reduced, mainly in the course of removal of the last of the ammonium cations from the samples.
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