Abstract
The thermal decomposition of K 3[Co(C 2O 4) 3]·3H 2O in the solid-state, was studied by thermogravimetry, high temperature reflectance spectroscopy, differential thermal analysis, mass spectrometry, gas evolution analysis, and by magnetic techniques. The stoichiometry of the decomposition reaction was determined and a mechanism is proposed to explain the reaction. The ultraviolet photolysis of the compound, in the solid-state, was also determined. The photolysis and thermal decomposition reactions did not involve exactly the same products.
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