Abstract
Polyfluoroalkyl iodides, such as Cl(CF2)nI(n=4, 6, 8, 1b-1d) and F(CF2)I (n=6, 8, 1e-1f) reacted with sodium sulfite in neutral aqueous DMF solution to give the corresponding sulfinates Cl(CF2)SO2Na (n=4, 6, 8, 2b-2d) and F(CF2)SO2Na (n=6, 8, 2e-2f) in moderate yields. I(CF2)2O(CF2)2SO2F ( la ) reacted under the same condition to give 3-oxaoctafiuoropentane-1,5-disulfinates (2a).
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