Abstract
The silanols formed on the cleavage of organosilyl protecting groups from organic compounds can be efficiently reconverted into the chlorosilanes used in the initial silylation reaction by treatment with SOCl 2. The silanol tBuMe 2SiOH is very readily removed from organic reaction mixtures as its remarkably volatile hemihydrate [ tBuMe 2SiOH] 2·H 2O.
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