Abstract
The porosity of co-precipitated iron(II) and nickel(II) oxalate samples was investigated after thermolysis at different temperatures. Specific surface area values of the obtained nickel(II) ferrite samples have been determined by means of the BET method. Maximal values of the specific surface area and pore volume have been fixed for ferrite samples obtained when the thermolysis of oxalates was carried at 500 °C during an hour. Specific surface value in this case was 335 m 2/g and pore volume 0.46 cm 3/g. At comparatively higher temperatures of thermal decomposition (600 °C) the indicated parameters of porous structure decrease sharply: specific surface area value to 20–25 m 2/g and pore volume – to 0.20 cm 3/g. A similar picture observed also when thermolysis was carried at 500 °C during 2 h. In this case specific surface area value decreases to 30 m 2/g and pore volume – to 0.22 cm 3/g.
Sign-in/Register to access full text options 
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
