Abstract

The orientation relationship between lath martensite and the narrow films of retained austenite in low carbon, low alloy steels has been determined to an accuracy of approximately ± 1 2° using Kikuchi line patterns obtained with a 7 nm probe in a 200 kV STEM set up for microdiffraction. The mean of the orientation relationship determinations was close to the Greninger-Troiano relationship with the extreme results showing a spread of ±2° and lying between the neighbouring Kurdjumov-Sachs and aishiyama-Wassermann relationships. Laths with the same habit plane formed packets and, in general, adjacent laths in such a packet were of the same orientation. However a few cases were observed where adjacent laths had markedly different orientations. In all these cases the two orientations represented a pair of orientation relationship variants in which the same close packed plane in the austenite was parallel to a close packed plane in the martensite and the same close packed direction in the austenite was approximately parallel to a close packed direction in the martensite, i.e. (111) γ nearly parallel to (101) α [11 10] γ 1.5 to 3° from [ 111] α and (111) γ nearly parallel to (101) α [1 10] γ 1.5 to 3° from [ 111]α . These two orientation relationship variants approximated to a twin relationship between the adjacent laths and in the less accurate conventional electron diffraction spot patterns could easily have been interpreted as a twin relationship. Single surface trace analysis showed that the long direction of the laths was always the [1 10] γ direction which is approximately 2.5° from [11 1] α , while the habit plane of the laths was consistent with (557) γ—i.e. an ( hhl) γ plane approximately 10° from the (111) γ which is parallel to (101) α.

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