Abstract
The influence of ethylene glycol (EG) on the preparation of K2SnSi3O9H2O (AV-6) was studied in this work. The EG content clearly changes the synthesis process. Although the morphology of the samples is similar, the products are mixtures containing AV-6, AV-7 (K 2 SnSi 3 O 9 ·H 2 ) and AV-11 (K f Sn 2 SiO 18 ). At high EG content, nano crystal of Sn-AV-11, instead of AV-6, is crystallized from the system. The samples were characterized by powder XRD, SEM, solid-state 29 Si MAS NMR spectroscopy and thermogravimetric (TG) analysis.
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
