Abstract
The gigapascal pressure thermal technique was described in detail as a new tool to produce new ternary metal hydrides. Thus, the occurrence of new phases in the A–Pd–H (A=Li, Na or Mg) system was investigated. The samples were subjected to pressures up to 6 GPa and subsequently heated up to 600 °C using LiAlH 4 as an internal hydrogen source. The reaction times were remarkably short as compared to conventional methods. The new phases were revealed by X-ray powder diffraction measurements showing that this technique is promising for producing new ternary metal hydrides.
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