The Effects of Food-Simulating Liquids on Surface Roughness, Surface Hardness, and Solubility of Bulk-Fill Composites

Abstract

Aim: To investigate the surface roughness, surface hardness, and solubility of bulk-fill composites after exposure to food-simulating liquids (FSLs). Materials and Methods: A total of 200 disc-shaped samples (8 mm diameter × 4 mm depth) were prepared using four bulk-fill composites (SonicFillTM, Tetric® EvoCeram Bulk Fill, Beautifil-Bulk Restorative, FiltekTM Bulk Fill Posterior Restorative) and a microhybrid composite (FiltekTM Z250) ( n = 40). Following the measurement of initial weights of the samples ( m1), the surface roughness measurements were gauged using a contact-profilometer. The samples were stored in four different FSLs for 7 days, and then the second surface roughness values were recorded. The samples were stored in a desiccator to reach the constant mass and the values were recorded as m2, then the solubility levels were calculated. The Vickers microhardness values of the samples were determined. A total of 20 specimens were evaluated in terms of surface morphology with a scanning electron microscope (SEM). Data were statistically analyzed with the two-way ANOVA and Bonferroni tests ( P < .05). Results: Beautifil-Bulk Restorative was affected at most in terms of surface roughness after storage in FSLs and citric acid caused the highest values in this group ( P < .005). Beautifil-Bulk Restorative and Filtek Z250 showed the highest surface hardness values, while the Tetric EvoCeram group had the lowest. The highest solubility values were found in Beautifil-Bulk Restorative, and citric acid and ethanol yielded the highest solubility values for all of the composites. Conclusion: Beautifil-Bulk Restorative is the most affected group in all parameters evaluated and also affected overly by citric acid among the FSLs in consequence of its prereacted glass ionomer fillers.