Abstract
In this chapter we present case studies showing how complementary in situ techniques including ambient pressure scanning tunneling microscopy, ambient pressure infrared reflection absorption spectroscopy, and ambient pressure X-ray photoelectron spectroscopy (AP-XPS) can be applied to study the dynamic oxide/metal interfaces formed on model heterogeneous catalyst surfaces. This approach helps to identify active local phases or structures on catalysts and critical adsorbate species during reaction conditions, thus guiding the determination of reaction mechanisms.
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