Abstract
The MoC phase with the WC structure was prepared by a novel synthetic route that involved the stoichiometric disproportionation of a high-temperature phase, Mo 3C2, to MoC and M02C at 1000 °C. MoC was found to be thermodynamically stable at temperatures below 1080 °C. From consideration of equilibrium and calorimetric data, the thermodynamic properties of MoC can be established as S298 0/R = 4.41(0.3) andΔH 298 0/R = -3430(800)K,
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