Abstract
Abstract The synthesis and thermal behavior of the new [Pd(fum)(bipy)] n ·2nH2O (1), [Pd(fum)(bpe)] n ·nH2O (2) and [Pd(fum)(pz)] n ·3nH2O (3) {bipy = 4,4′-bipyridine, bpe = 1,2-bis(4-pyridyl)ethene and pz = pyrazine} fumarate complexes are described in this work as well their characterization by IR and 13C CPMAS NMR spectroscopies. TG curves showed that the compounds released organic ligands and lattice water molecules in the temperature range of 46–491 °C. In all the cases, metallic palladium was identified as the final residue.
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