Abstract
AbstractPoly(methyl acrylate)s, poly(ethyl acrylate)s, and poly(butyl acrylate)s with α,ω‐di(bromo) chain ends and Mn from 8500 to 35,000 were synthesized by single‐electron‐transfer living radical polymerization (SET‐LRP). The analysis of their chain ends by a combination of 1H and 2D‐NMR, GPC, MALDI‐TOF MS, chain end functionalization, chain extension, and halogen exchange experiments demonstrated the synthesis of perfectly bifunctional polyacrylates by SET‐LRP. © 2007 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 45: 4684–4695, 2007
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