Abstract
(±) Hydroxytremetone (III) has been synthesized from 2-(α-hydoxyisopropyl)-6-hydroxy-coumaran (V b) via its 0-acetate V c by dehydration with phosphorus tribromide in pyridine solution, followed by acylation with a mixture of trifluoroacetic anhydride and acetic acid. Isohydroxytremetone (IX b) was also synthesized.
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