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https://doi.org/10.1021/jo5023537
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Cite Journal: The Journal of Organic Chemistry |  Publication Date: Nov 17, 2014 |
 Citations: 28 |  License type: cc-by-nc |
A method for the synthesis of gem-difluorinated nitroso compounds is described. The reaction involves interaction of organozinc reagents with (bromodifluoromethyl)trimethylsilane followed by nitrosation of difluorinated organozinc species with an n-butyl nitrite/chlorotrimethylsilane system.
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