Abstract
A series of semifluorinated fluorocarbon/hydrocarbon di- and triblock copolymers were prepared by atom transfer radical polymerization (ATRP). The mono- and difunctional macroinitiators, which were obtained from bulk ATRP of styrene, butyl acrylate and methyl acrylate, initiated solution ATRP of 2-[(perfluorononenyl)oxy]ethyl methacrylate and ethylene glycol mono-methacrylate mono-perfluorooctanoate, respectively. The formation of the block copolymer was confirmed with size exclusion chromatography and 1H NMR spectrum.
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