Abstract

采用模板法、离子交换法、沉淀法和浸渍法等多步反应合成了系列CdS/Al-HMS和负载的Pt/CdS/Al-HMS光催化复合材料;利用XRD、TEM、XRF及UV-Vis漫反射光谱等分析技术对其进行了表征;研究结果表明:CdS的复合量是影响CdS/Al-HMS复合材料结构的主要因素.当CdS复合量较低时,形成掺杂复合材料;当CdS复合量较高时,形成纳米复合材料.载6%Pt后的CdS/Al-HMS光催化复合材料降解甲酸的最高产氢速率为22.3mL/h,420nm处的表观量子产率为12%.

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