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https://doi.org/10.1039/d1ob02277f
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Cite Journal: Organic & Biomolecular Chemistry |  Publication Date: Jan 1, 2022 |
 Citations: 2 |
Affiliation: Nara Women's University
1,1-Disubstituted alkenes feature high steric hindrance, which renders their Wacker-type oxidation difficult. We demonstrate the stereoselective synthesis of 2-hydroxytetrahydrofurans via the Wacker-type oxidation of 3-methyl-3-buten-1-ols by using a PdCl2(MeCN)2/NO/BQ catalyst system under 1 atm O2 in H2O or H2O/DMF.
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