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Abstract
One polyoxometalate-based silver(I) compound [Ag(2,2'-Bipy)2]3(PW12O40) (I) (2,2'-Bipy = 2,2'- bipyridine) has been synthesized and structurally characterized by IR spectroscopy, elemental analysis, XRPD and X-ray single-crystal structure analysis (CIF file CCDC no. 1572216). Compound I exhibits a crystalline three-dimentional supramolecular framework constructed by Ag-2,2'-Bipy coordination units and [PW12O40]3− template anions, in which there are multiform π...π interactions and hydrogen bonds. The cyclic voltammetric experiments show that compound I displays a good electrocatalytic activity toward the reduction of nitrite.
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