Synthesis, characterization and 2,5-pyridinedicarboxylic acid interaction of Zinc(II) complexes with N-(4-X-phenyl)pyridine-2-yl-methanimine ligands (X= -Cl and -N(CH3)2)

Nicole Dinamarca ,P.i Levin ,Manuel Azócar ,Hugo Muñoz

doi:10.21060/cis.v5i2.2692

Synthesis, characterization and 2,5-pyridinedicarboxylic acid interaction of Zinc(II) complexes with N-(4-X-phenyl)pyridine-2-yl-methanimine ligands (X= -Cl and -N(CH3)2)

Nicole Dinamarca , P.i Levin + Show 2 more

https://doi.org/10.21060/cis.v5i2.2692

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Journal: Communications In Inorganic Synthesis

Publication Date: Nov 13, 2017

Affiliation: University of Santiago Chile

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Abstract

Abstract: Two new Zn(II) N-(4-X-phenyl)pyridine-2-yl-methanimine complexes, [Zn(NN´-Cl)Cl 2 ]( 1 ) and [Zn(NN´-N(CH 3 ) 2 )Cl 2 ]( 2 ), have been synthesized and characterized by elemental analysis, FT-IR and NMR- 1 H spectra. The crystal structure of complex 1 was determined by X-ray single crystal diffraction. Experiments performed by Benesi-Hilderbrand method indicate that zinc complexes interact with 2,5-pyridinedicarboxyc acid.

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