Abstract
Reactions of Nb 6 I 11 or of Nb 3 I 8 plus niobium with sulfur in a sealed niobium container afford Nb 6 I 9 S in high yield. The latter takes up hydrogen to form Nb 6 (H)I 9 S, the hydrogen presumably bonding within the metal cluster as in other niobium iodide cluster examples. The closely related structures were both refined in P1 by single-crystal X-ray diffraction
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