Abstract
Reaction of (μ 3-S)FeCo2(CO)9 with N-substituted bis(diphenylphosphanyl)amine Ph2PN(R)PPh2 (R = CH2CH2CH3, A; CH2Ph, B) at room temperature in CH2Cl2 afforded dicobalt–iron cluster complexes (μ 3-S)FeCo2(CO)7[Ph2PN(R)PPh2] (R = CH2CH2CH3, 1; CH2Ph, 2) in 75% and 66% yields, respectively. 1 and 2 were characterized by elemental analysis and spectroscopy. In addition, the molecular structures of A, 1, and 2 were determined by single crystal X-ray diffraction analysis.
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