Abstract
AbstractSingle crystals of [Fe(Cp)2]3(Bi2Cl9)·thf were obtained from a thf solution containing ferrocene and BiCl3. The structure shows disorder at room temperature which disappears upon cooling, coupled with a decrease in symmetry. The title compound crystallizes in the orthorhombic space group P212121 [a = 1698.64(2), b = 2318.69(3), c = 1085.66(2) pm] with three ferrocenium ions, one nonachlorodibismutate ion and one molecule of thf in the asymmetric unit.
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