Abstract
A novel chiral poly(amide imide) containing L-alanine was synthesized by direct polycondensation reaction of newly synthesized N,Nâ-(4,4â-diphthaloyl)-bis-L-alanine diacid with 4,4â-diaminodiphenyl ether in a medium consisting of N-methyl-2-pyrrolidone (NMP), triphenylphosphite (TPP), calcium chloride (CaCl2), and pyridine. The new chiral diimide-diacid monomer was synthesized by direct reaction of 3,3â-4,4â-Biphenyl tetracarboxylic acid dianhydride with L-alanine in acetic acid under reďŹuxing conditions. The resulting compounds were obtained in quantitative yields and high purity. The synthetic diacid monomer was characterized by elemental analysis, 1H-NMR spectroscopy, FT-IR techniques and speciďŹc rotation, the obtained polymer was characterized by FTIR techniques, speciďŹc rotation and solubility testing.
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