Abstract
Methyldiethoxistibane and maleic or phthalic acid in a ratio of 1:1 in ethanolic solution at -78 °C react to give methyl(maleato)stibane (1) and methyl(phthalato)stibane (2) respectively. At room temperature polymeric compounds of the same analytical composition are obtained (1a and 2a). The crystal structure of the solid methyl(phthalato)stibane 2 was determined by X-ray diffraction. It shows that the central antimony atom is hexacoordinated by addition of a solvate ethanol. The correct formula for the solid should be
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