Abstract
Tetraphenylantimony N-benzoylglycinate (I) has been synthesized by the reaction between pentaphenylantimony and N-benzoylglycine in toluene. According to X-ray diffraction data, the antimony atom in a molecule of complex I has a trigonal bipyramidal coordination to the oxygen atom in axial position. The Sb‒Ceq, Sb‒Cax, and Sb‒O bond lengths are 2.116(6)‒2.138(6), 2.183(6), and 2.200(4) A, respectively. The intramolecular Sb⋯O=C distance between the carbonyl oxygen atom and the central antimony atom is 3.35(2) A.
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