Abstract

1,1,2,2-tetrachlorodisilane was prepared from 1,1,2,2-tetramesityldisilane by reaction with liquid HCl, 1,1,2,2-tetrafluorodisilane by fluorination of tetrabromodisilane with ZnF 2. With PCl 5, 1,1,2,2-tetramesityldisilane was easily chlorinated to form 1,2-dichlorotetramesityldisilane but the subsequent reduction with LiAlD 4 was not successful. The 29Si-NMR, Infrared and Raman spectra are reported.

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