Abstract

The investigation of changes in physical properties, mechanical properties, and microscopic pore structure characteristics of tight sandstone after high-temperature heat treatment provides a theoretical basis for plugging removal and stimulation techniques, such as high energy gas fracturing and explosive fracturing. In this study, core samples, taken from tight sandstone reservoirs of the Yanchang Formation in the Ordos Basin, were first heated to different temperatures (25-800°C) and then cooled separately by two distinct cooling methods—synthetic formation water cooling and natural cooling. The variations of wave velocity, permeability, tensile strength, uniaxial compressive strength, and microscopic pore structure of the core samples were analyzed. Experimental results demonstrate that, with the rise of heat treatment temperature, the wave velocity and tensile strength of tight sandstone decrease nonlinearly, yet its permeability increases nonlinearly. The tight sandstone’s peak strength and elastic modulus exhibit a trend of the first climbing and then declining sharply with increasing temperature. After being treated by heat at different temperatures, the number of small pores varies little, but the number of large pores increases obviously. Compared to natural cooling, the values of physical and mechanical properties of core samples treated by synthetic formation water cooling are apparently smaller, whereas the size and number of pores are greater. It can be explained that water cooling brings about a dramatic reduction of tight sandstone’s surface temperature, generating additional thermal stress and intensifying internal damage to the core. For different cooling methods, the higher the core temperature before cooling, the greater the thermal stress and the degree of damage caused during the cooling process. By taking into consideration of changes in physical properties, mechanical properties, and microscopic pore structure characteristics, the threshold temperature of tight sandstone is estimated in the range of 400-600°C.

Highlights

  • With the further exploitation of oilfields, coal mines, and geothermal energy and the increasing operations under the deep geological conditions, the research on change in rock properties after high-temperature heat treatment attracts great attention [1]

  • Due to the limited core samples, the normalization method has been applied to exclude the influences of physical properties and mineral compositions of different core samples on acoustic wave velocity: a = Si × 100%, ð5Þ

  • A series of tests have been carried out to study the effect of high-temperature heat treatment on the physical properties, mechanical properties, and microscopic pore structure of tight sandstone under synthetic formation water cooling and natural cooling

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Summary

Introduction

With the further exploitation of oilfields, coal mines, and geothermal energy and the increasing operations under the deep geological conditions, the research on change in rock properties after high-temperature heat treatment attracts great attention [1]. As the development techniques advance, the phenomenon that the formation is first heated up and cooled down in a quick manner takes place in the processes of the combined perforation and hydraulic fracturing and the high energy gas fracturing and plugging removal followed by water injection For this reason, it is of great importance to study the changes in pores and permeability of hightemperature rock after water cooling [2]. In the course of high-temperature heat treatment or cooling of tight sandstone, physicochemical changes occur to some extent, giving rise to a dramatic change in the internal structure of the sandstone and sophisticating its physical and mechanical properties [25]. The changes and evolution characteristics of microscopic structures at different scales are identified with different cooling methods and at various temperatures, aiming at providing a theoretical basis for the high energy gas or explosive fracturing and the combined perforation and hydraulic fracturing technique in tight sandstone reservoirs

Experimental Section
H27-1 H27-2 H27-3 H28-1 H28-2 H28-3 H29-1 H29-2 H29-3 H30-1 H30-2 H30-3
Results and Discussion
Conclusions
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