Abstract
The strengths of the gel effect, and the monomer conversions at which the gel effect sets in for the polymerizations of some methacrylic acid esters, were determined at different temperatures from the courses of polymerization measured by differential scanning calorimetry. It was found that the strength of the gel effect is greatly influenced by the reaction temperature and the ester residue in the molecule of the monomer, whereas the “critical” conversion for individual monomers is practically independent of the reaction temperature in the measured interval, but is strongly dependent on the length of the ester residue.
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