Abstract
Abstract The title compound crystallizes monoclinicly in the space group P21/c with lattice parameters a = 13.522 Å, b = 22.379 Å, c = 15.071 Å und β = 95.95°. In the polyanion two α-PW9O34 moieties are bridged by two octahedral WO6 units. A potassium ion in the central cavity is surrounded by eight oxygen atoms of the polyanion in hexagonal bipyramidal coordination. - The vibration spectrum of the solid and its aqueous solution are discussed.
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