Abstract
A novel cadmium cyclohexaphosphate (C5H14N2)2Cd2Cl2P6O18.4H2O has been prepared and characterized by single-crystal X-ray diffraction, infrared and Raman spectroscopies, thermogravimetric analysis, and cyclic voltammetry. The structure consists of vertex linked of CdO5Cl octahedral and P6O18 rings assembled into a two-dimensional macroanionic layers. Organic double-protonated homopiperazine cations are located between these layers and interact with the framework both electrostatically and via hydrogen bonds of N–H···O(Cl). [Supplemental materials are available for this article. Go to the publisher's online edition of Phosphorus, Sulfur, and Silicon and the Related Elements to view the following free supplemental files: Additional figures]
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