Abstract
We have studied the effect of sintering temperature on the structural and phase transformations of alloys produced by the spark plasma sintering of Ti + 23.5 at % Al + 21 at % Nb powder mixtures at temperatures in the range 1100–1550°C. The sintered alloys have been characterized by X-ray diffraction, scanning electron microscopy, and energy dispersive X-ray spectroscopy (elemental X-ray mapping). The alloys sintered at temperatures of 1100 and 1200°C have been shown to have a nonuniform microstructure. According to electron microscopy results, the alloys consist of grains of the α2 and Nb2Al phases and small precipitates of the O-phase (intermetallic compound Ti2AlNb). In addition, there are particles of unreacted niobium and titanium. The alloys sintered at a temperature of 1300°C have a uniform lamellar structure.
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