Abstract
This work reports the development of very low residual stress and low strain gradient polycrystalline SiC (poly-SiC) thin films deposited by low pressure chemical vapor deposition (LPCVD). Using dichlorosilane (DCS, SiH <sub xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">2</sub> Cl <sub xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">2</sub> ) and acetylene (C <sub xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">2</sub> H <sub xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">2</sub> ) as precursors, it was found that the flow rate of DCS can be used to adjust the residual stress from tensile to compressive in as-deposited films. The resulting poly-SiC films, with tensile stresses lower than 50 MPa and strain gradients as low as 1.3times10 <sup xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">-4</sup> mum <sup xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink">-1</sup> , are well-suited for MEMS and NEMS structural materials.
Published Version
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