Abstract
Nano-particles of two new Cd(II) supramolecular complexes, [Cd(4,4-di-tert-bubipy)Cl2(DMSO)] (1) and [CdI2(4,4′-dmbpy)(DMSO)] (2) have been synthesized by sonochemical process and characterized by scanning electron microscopy, X-ray powder diffraction, IR spectroscopy and elemental analyses. The structure of compound 1 has been characterized by single crystal X-ray diffraction. The prepared nano-structure was characterized by scanning electron microscopy and X-ray powder diffraction. The nano-structures of supramolecular complexes have been synthesized with calcination of complexes at oleic acid as a surfactant at 190 oC too. The size of the samples prepared by sonochemical method and calcination are about 30–40 and 40–50 nm respectively.
Sign-in/Register to access full text options 
Free) 
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a call
