Abstract
AbstractElectrochemical characterization of palladium nanoparticles surrounded by a palladium oxide shell (Pd@PdO) is described from a combination of voltammetry plus electrochemical quartz crystal microbalance experiments at nanoparticle deposits on graphite electrodes in contact with aqueous H2SO4 and NaOH solutions. A method for determining the metal core size and oxide shell thickness of the Pd@PdO nanoparticles, based on a combination of conventional voltammetry of nanoparticles in DMSO solution and voltammetry of nanoparticle deposits in contact with 0.10 M aqueous NaOH solution, is described.
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