Abstract

The use of sulfonates as traceless linkers was demonstrated. Resin-bound biphenylsulfonates 3 were prepared from hydroxyethyl­methyl resin 1 in two steps. The reactions of 3 with Grignard reagents were performed in the presence of a nickel catalyst to give unfunctionalized terphenyls in 55-66% yield (from 2, 8 examples).

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