Abstract
There is a need for low-cost, high-accuracy measurement of water content in various materials. This study assesses the performance of a new microwave swept frequency domain instrument (SFI) that has promise to provide a low-cost, high-accuracy alternative to the traditional and more expensive time domain reflectometry (TDR). The technique obtains permittivity measurements of soils in the frequency domain utilizing a through transmission configuration, transmissometry, which provides a frequency domain transmissometry measurement (FDT). The measurement is comparable to time domain transmissometry (TDT) with the added advantage of also being able to separately quantify the real and imaginary portions of the complex permittivity so that the measured bulk permittivity is more accurate that the measurement TDR provides where the apparent permittivity is impacted by the signal loss, which can be significant in heavier soils. The experimental SFI was compared with a high-end 12 GHz TDR/TDT system across a range of soils at varying soil water contents and densities. As propagation delay is the fundamental measurement of interest to the well-established TDR or TDT technique; the first set of tests utilized precision propagation delay lines to test the accuracy of the SFI instrument’s ability to resolve propagation delays across the expected range of delays that a soil probe would present when subjected to the expected range of soil types and soil moisture typical to an agronomic cropping system. The results of the precision-delay line testing suggests the instrument is capable of predicting propagation delays with a RMSE of +/−105 ps across the range of delays ranging from 0 to 12,000 ps with a coefficient of determination of r2 = 0.998. The second phase of tests noted the rich history of TDR for prediction of soil moisture and leveraged this history by utilizing TDT measured with a high-end Hewlett Packard TDR/TDT instrument to directly benchmark the SFI instrument over a range of soil types, at varying levels of moisture. This testing protocol was developed to provide the best possible comparison between SFI to TDT than would otherwise be possible by using soil moisture as the bench mark, due to variations in soil density between soil water content levels which are known to impact the calibration between TDR’s estimate of soil water content from the measured propagation delay which is converted to an apparent permittivity measurement. This experimental decision, to compare propagation delay of TDT to FDT, effectively removes the errors due to variations in packing density from the evaluation and provides a direct comparison between the SFI instrument and the time domain technique of TDT. The tests utilized three soils (a sand, an Acuff loam and an Olton clay-loam) that were packed to varying bulk densities and prepared to provide a range of water contents and electrical conductivities by which to compare the performance of the SFI technology to TDT measurements of propagation delay. For each sample tested, the SFI instrument and the TDT both performed the measurements on the exact same probe, thereby both instruments were measuring the exact same soil/soil-probe response to ensure the most accurate means to compare the SFI instrument to a high-end TDT instrument. Test results provided an estimated instrumental accuracy for the SFI of +/−0.98% of full scale, RMSE basis, for the precision delay lines and +/−1.32% when the SFI was evaluated on loam and clay loam soils, in comparison to TDT as the bench-mark. Results from both experiments provide evidence that the low-cost SFI approach is a viable alternative to conventional TDR/TDT for high accuracy applications.
Highlights
Accurate measurement of moisture content is a key requirement in hydrological, geophysical and bio-geochemical research as well as for material characterization, process control and irrigation efficiency in water limited regions
The most logical pathway to enhanced accuracy lies in a transition from time-domain based TDR measurements towards a frequency-domain based network analyzer style measurement of the bulk complex permittivity that will allow for removal of the adverse effects that high surface area soils and electrical-conductivity, due to elevated soil-salinity, imparts onto the measurements of apparent bulk permittivity that is utilized in the traditional TDR approach
The results of the precision delay line testing of the swept frequency domain instrument (SFI) instrument are shown in Figure 3 and resulted in a root-mean-squared error (RMSE) of 105 ps for propagation delay across the span of 0 to
Summary
Accurate measurement of moisture content is a key requirement in hydrological, geophysical and bio-geochemical research as well as for material characterization, process control and irrigation efficiency in water limited regions Within these areas, consideration of the surface area and associated bound water content [1] is becoming increasingly important for providing answers to many fundamental questions ranging from characterization of cotton fiber maturity, to accurate dielectric measurement methods of soil water content for hydrological assessment and efficient irrigation practices. One promising technique to address the increasing demands for higher accuracy water content measurements is the utilization of electrical permittivity characterization of materials as a proxy for water content. This proxy has enjoyed a strong following in the soil-science and geological community through measurements of apparent bulk permittivity via time-domain-reflectometry (TDR) as well in many process control applications. The most logical pathway to enhanced accuracy lies in a transition from time-domain based TDR measurements towards a frequency-domain based network analyzer style measurement of the bulk complex permittivity that will allow for removal of the adverse effects that high surface area soils and electrical-conductivity, due to elevated soil-salinity, imparts onto the measurements of apparent bulk permittivity that is utilized in the traditional TDR approach
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