Abstract
Single crystals KxFexSn8−xO16 (KFSO, x~1.98) were grown by the flux slow cooling method. Needle like single crystal having 120μm width and 3mm length at a maximum was obtained by slow cooling to 1000°C at a rate of 2°Ch−1 using starting materials with a 40mol% crystal composition of (K2O)1(Fe2O3)1(SnO2)1 and a 60% flux composition of (K2O)2(MoO3)1(B2O3)1. KFSO single crystal was refined and calculated atomic coordination, bond length and so on from the x-ray diffraction method. Final R and wR values showed 2.24% and 6.23%, respectively.
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