Shear bond strength of veneering porcelain to zirconia: Effect of surface treatment by CNC-milling and composite layer deposition on zirconia

Abstract

ObjectivesThe purpose of this study was to evaluate the shear bond strength of veneering feldspathic porcelain to zirconia substrates modified by CNC-milling process or by coating zirconia with a composite interlayer. MethodsFour types of zirconia–porcelain interface configurations were tested: RZ – porcelain bonded to rough zirconia substrate (n=16); PZ – porcelain bonded to zirconia substrate with surface holes (n=16); RZI – application of a composite interlayer between the veneering porcelain and the rough zirconia substrate (n=16); PZI – application of a composite interlayer between the porcelain and the zirconia substrate treated by CNC-milling (n=16). The composite interlayer was composed of zirconia particles reinforced porcelain (30%, vol%). The mechanical properties of the ceramic composite have been determined. The shear bond strength test was performed at 0.5mm/min using a universal testing machine. The interfaces of fractured and untested specimens were examined by FEG-SEM/EDS. Data was analyzed with Shapiro–Wilk test to test the assumption of normality. The one-way ANOVA followed by Tukey HSD multiple comparison test was used to compare shear bond strength results (α=0.05). ResultsThe shear bond strength of PZ (100±15MPa) and RZI (96±11MPa) specimens were higher than that recorded for RZ (control group) specimens (89±15MPa), although not significantly (p>0.05). The highest shear bond strength values were recorded for PZI specimens (138±19MPa), yielding a significant improvement of 55% relative to RZ specimens (p<0.05). SignificanceThis study shows that it is possible to highly enhance the zirconia–porcelain bond strength – even by ~55% – by combining surface holes in zirconia frameworks and the application of a proper ceramic composite interlayer.