Abstract
The gas chromatographic analysis of NaBH4-reduced monosaccharide mixtures (either trimethylsilylated or acetylated) and NaBH4-reduced trimethylsilylated disaccharide mixtures in open tubular glass capillary columns is described. Complete separations of the investigated monosaccharides can be achieved if the same separation column and the appropriate method of derivatization are used. Kovats' retention indices of the derivatives are determined and their experimental repeatability is discussed.
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