Abstract
The rate of protium-deuterium exchange, catalyzed by deuterated Raney nickel in deuterium oxide, in various positions in methyl glycopyranosides and furanosides has been studied. In general, the exchange process is not highly regio-selective in these compounds. However, conditions were found under which methyl β- d-fructopyranoside can be selectively labelled on C-5, methyl β- d-fructofuranoside on C-3, and methyl β- d-galactopyranoside on C-3 and C-4.
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